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[Application](±)-N,N'-Bis(alpha-methylbenzyl) sulfamide

관리자 | 2017.07.03 11:43 | 조회 4007

(±)-N,N'-Bis(alpha-methylbenzyl) sulfamide

COMPOUND IDENTIFICATION

Compound Name (±)-N,N'-Bis(alpha-methylbenzyl) sulfamide

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

50 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / ethanol = 80 / 20

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

5

Injection amount (mg)

0.02

Temperature (°C)

25

Pressure (MPa)

 

Detection

UV 220 nm

Elution order

 

No.

Rt

K’

1

0.31

1.73

2

0.44

2.84

 

Alpha Value

Resolution

1 - 2

1.64

3.08








(±)-N,N'-Bis(alpha-methylbenzyl) sulfamide

COMPOUND IDENTIFICATION

Compound Name (±)-N,N'-Bis(alpha-methylbenzyl) sulfamide

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

150 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / 2-propanol = 80 / 20

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.001

Temperature (°C)

25

Pressure (MPa)

 

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

4.48

1.63

2

4.91

1.88

 

Alpha Value

Resolution

1 - 2

1.15

2.68









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