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[Application]Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

관리자 | 2017.07.28 11:42 | 조회 5049
APPLICATION ID 1269

Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

COMPOUND IDENTIFICATION

Compound Name Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® AY-H

250 x 4.6mm / 5µm

Mobile Phase Composition

CO2 / 2-propanol = 85 / 15

Chromatographic Mode

SFC

Flow rate (ml/min)

3

Injection amount (mg)

 

Temperature (°C)

RT

Pressure (MPa)

12

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

4.23

3.23

2

7.48

6.48

 

Alpha Value

Resolution

1 - 2

2.01

10.71

 

 

 

 

 

 

 


APPLICATION ID 1270

Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

COMPOUND IDENTIFICATION

Compound Name Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® AY-H

250 x 4.6mm / 5µm

Mobile Phase Composition

CO2 / methanol = 85 / 15

Chromatographic Mode

SFC

Flow rate (ml/min)

3

Injection amount (mg)

 

Temperature (°C)

RT

Pressure (MPa)

12

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

3.05

2.05

2

3.69

2.69

 

Alpha Value

Resolution

1 - 2

1.31

4.28









APPLICATION ID 1271

Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

COMPOUND IDENTIFICATION

Compound Name Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALCEL® OZ-H

250 x 4.6mm / 5µm

Mobile Phase Composition

CO2 / 2-propanol = 85 / 15

Chromatographic Mode

SFC

Flow rate (ml/min)

3

Injection amount (mg)

 

Temperature (°C)

RT

Pressure (MPa)

12

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

5.6

4.6

2

8.71

7.71

 

Alpha Value

Resolution

1 - 2

1.68

8.74










APPLICATION ID 1272

Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

COMPOUND IDENTIFICATION

Compound Name Methyl 1-benzyl-5-oxo-3-pyrrolidinecarboxylate

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALCEL® OZ-H

250 x 4.6mm / 5µm

Mobile Phase Composition

CO2 / methanol = 85 / 15

Chromatographic Mode

SFC

Flow rate (ml/min)

3

Injection amount (mg)

 

Temperature (°C)

RT

Pressure (MPa)

12

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

4.05

3.05

2

5.77

4.77

 

Alpha Value

Resolution

1 - 2

1.56

8.2











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